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Abstract Recently, additive manufacturing (AM) fabrications are commonly applied to produce acoustic metamaterials or phononic crystals (PnCs) as tools for complex geometrical designs. However, the material properties of those additive manufactured materials are less involved in the core portion of those PnC designs. Here we report a purely materials-driven, temperature switchable PnC in which Bragg gaps appear or vanish as the lattice medium toggles between liquid water and solid ice. Six widely used AM polymers were acoustically characterized, where stereolithography (SLA) resins showed an impedance mismatch of ≈50% with water but <1% with ice, whereas inkjet agar gel exhibited the opposite trend. A 10 × 10 SLA resin PnC therefore displayed >20 dB on/off contrast at 145 kHz and around 300 kHz when cycled across 0 °C, confirmed experimentally and with plane wave and simulation models. Unlike previous thermally tuned PnCs that depend on volumetric swelling or liquid metal infiltration, the present approach preserves geometry, requires no external actuators and operates with sub 1 °C stability. This simple, robust strategy lays the foundation for band pass filters, steerable lenses and non-reciprocal acoustic circuits that can be frozen or thawed on demand. 

The principle of the conventional ultrasound test states that the detectable voids cannot be smaller than the acoustic wavelength. However, by using effective medium approximation, the fraction of small voids can be estimated by the variation of the effective density. In this study, a non-contacting ultrasound-based porosity fraction mapping methodology is developed for estimated small voids in coal with long operating wavelength in air. This novel ultrasonic technique based on the mechanical properties of coal offers a rapid scan of the effective density mapping and distribution of void fraction over a large sample area, which overcame the limitation of small voids detection in the conventional ultrasound testing. 

The functionality of thermally active phononic crystals (PnC) and metamaterials can be greatly enhanced by utilizing the temperature-dependent physical characteristics of heat-sensitive materials within the periodic structure. The phase transformation between water and ice occurs within a narrow range of temperatures that can lead to significant changes in its acoustic transmission due to the modification of the elastic properties of periodic phononic structures in an aqueous medium. A phononic crystal with acrylic scatterers in water is designed to function as an acoustic filter, beam splitter, or lensing based on the device’s temperature due to changes in the phase of the ambient medium. The transition from room temperature to freezing point reduces the contrast in acoustic properties between the ice-lattice and the scatterer materials (acrylic) and switches off the metamaterial of the water-based PnC. The numerically simulated equi-frequency contours and wave propagation characteristics demonstrate the switchable meta-material to the periodic phononic structure’s normal behavior due to the phase transition of water. Effects such as Van Hove’s singularity and filamentation-like effects in an acoustic meta-material system can be thermally tuned. 

Abstract In recent research, additions of solute to Ti and some Ti-based alloys have been employed to produce equiaxed microstructures when processing these materials using additive manufacturing. The present study develops a computational scheme for guiding the selection of such alloying additions, and the minimum amounts required, to effect the columnar to equiaxed microstructural transition. We put forward two physical mechanisms that may produce this transition; the first and more commonly discussed is based on growth restriction factors, and the second on the increased freezing range effected by the alloying addition coupled with the imposed rapid cooling rates associated with AM techniques. We show in the research described here, involving a number of model binary as well as complex multi-component Ti alloys, and the use of two different AM approaches, that the latter mechanism is more reliable regarding prediction of the grain morphology resulting from given solute additions. 

Abstract Rapid thermokinetics associated with laser-based additive manufacturing produces strong bulk crystallographic texture in the printed component. The present study identifies such a bulk texture effect on elastic anisotropy in laser powder bed fused Ti6Al4V by employing an effective bulk modulus elastography technique coupled with ultrasound shear wave velocity measurement at a frequency of 20 MHz inside the material. The combined technique identified significant attenuation of shear velocity from 3322 ± 20.12 to 3240 ± 21.01 m/s at 45 $$^\circ$$ ∘ and 90 $$^\circ$$ ∘ orientations of shear wave plane with respect to the build plane of printed block of Ti6Al4V. Correspondingly, the reduction in shear modulus from 48.46 ± 0.82 to 46.40 ± 0.88 GPa was obtained at these orientations. Such attenuation is rationalized based on the orientations of $$\alpha ^\prime$$ α ′ crystallographic variants within prior columnar $$\beta$$ β grains in additively manufactured Ti6Al4V. 

The advent of 3D digital printers has led to the evolution of realistic anatomical organ shaped structures that are being currently used as experimental models for rehearsing and preparing complex surgical procedures by clinicians. However, the actual material properties are still far from being ideal, which necessitates the need to develop new materials and processing techniques for the next generation of 3D printers optimized for clinical applications. Recently, the voxelated soft matter technique has been introduced to provide a much broader range of materials and a profile much more like the actual organ that can be designed and fabricated voxel by voxel with high precision. For the practical applications of 3D voxelated materials, it is crucial to develop the novel high precision material manufacturing and characterization technique to control the mechanical properties that can be difficult using the conventional methods due to the complexity and the size of the combination of materials. Here we propose the non-destructive ultrasound effective density and bulk modulus imaging to evaluate 3D voxelated materials printed by J750 Digital Anatomy 3D Printer of Stratasys. Our method provides the design map of voxelated materials and substantially broadens the applications of 3D digital printing in the clinical research area.